Information card for entry 7033322

Structure parameters

• Common name: [Ni2(LClO-tmpa)Cl2(H2O)(MeOH)]ClO4.xH2O
• Formula: C132 H144 Cl16 N24 Ni8 O33
• Calculated formula: C132 H144 Cl16 N24 Ni8 O33
• Title of publication: Magnetic and structural properties of dinuclear singly bridged-phenoxido metal(ii) complexes.
• Authors of publication: Massoud, Salah S.; Spell, Mark; Ledet, Catherine C.; Junk, Thomas; Herchel, Radovan; Fischer, Roland C.; Trávníček, Zdeněk; Mautner, Franz A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 5
• Pages of publication: 2110 - 2121
• a: 10.356 ± 0.0005 Å
• b: 19.7894 ± 0.0009 Å
• c: 19.0876 ± 0.0009 Å
• α: 90°
• β: 96.752 ± 0.002°
• γ: 90°
• Cell volume: 3884.7 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.078
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.1203
• Weighted residual factors for all reflections included in the refinement: 0.1381
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No