Information card for entry 7033660

Structure parameters

• Formula: C73 H107 Al4 Li4 N12 O8.5
• Calculated formula: C73 H107 Al4 Li4 N12 O8.5
• Title of publication: Multiple deprotonation of primary aromatic diamines by LiAlH4.
• Authors of publication: Less, Robert J.; Allen, Lucy K.; Steiner, Alexander; Wright, Dominic S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 9
• Pages of publication: 4141 - 4147
• a: 15.8568 ± 0.0005 Å
• b: 25.4155 ± 0.0009 Å
• c: 20.1493 ± 0.0008 Å
• α: 90°
• β: 101.022 ± 0.002°
• γ: 90°
• Cell volume: 7970.6 ± 0.5 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1082
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for significantly intense reflections: 0.1567
• Weighted residual factors for all reflections included in the refinement: 0.1814
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No