Information card for entry 7033662

Structure parameters

• Formula: C33 H47 Al Li N7 O
• Calculated formula: C33 H47 Al Li N7 O
• Title of publication: Multiple deprotonation of primary aromatic diamines by LiAlH4.
• Authors of publication: Less, Robert J.; Allen, Lucy K.; Steiner, Alexander; Wright, Dominic S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 9
• Pages of publication: 4141 - 4147
• a: 34.6994 ± 0.0004 Å
• b: 14.6711 ± 0.0002 Å
• c: 30.4757 ± 0.0004 Å
• α: 90°
• β: 120.945 ± 0.001°
• γ: 90°
• Cell volume: 13306.2 ± 0.3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1269
• Residual factor for significantly intense reflections: 0.0811
• Weighted residual factors for significantly intense reflections: 0.2375
• Weighted residual factors for all reflections included in the refinement: 0.2611
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No