Information card for entry 7033709

Structure parameters

• Formula: C38 H22 O12 P2 W2
• Calculated formula: C38 H22 O11.95 P2 W2
• Title of publication: 6-Methoxy-5-phosphaphenanthrene: a molecule with an unreactive P[double bond, length as m-dash]C double bond.
• Authors of publication: Wang, Lili; Wang, Zhihua; Wang, Qiuyan; Duan, Zheng; Mathey, François
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 8
• Pages of publication: 3717 - 3719
• a: 11.5815 ± 0.0007 Å
• b: 13.2137 ± 0.0007 Å
• c: 14.4201 ± 0.001 Å
• α: 63.056 ± 0.006°
• β: 74.408 ± 0.005°
• γ: 84.555 ± 0.005°
• Cell volume: 1893.9 ± 0.2 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291.15 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1055
• Residual factor for significantly intense reflections: 0.0741
• Weighted residual factors for significantly intense reflections: 0.1825
• Weighted residual factors for all reflections included in the refinement: 0.2109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No