Information card for entry 7033839

Structure parameters

• Formula: C32 H46 Li2 N8 Si2
• Calculated formula: C32 H46 Li2 N8 Si2
• SMILES: [Li]123[n]4c(C)ccc5cccc([N]61C(=[N]([Si](C)(C)C)[Li]16[n]6c(C)ccc7cccc([N]21C(=[N]3[Si](C)(C)C)N(C)C)c67)N(C)C)c45
• Title of publication: Inserted products of lithium silylquinolylamide dimers [{8-(2-R-C9H5N)N(Me3Si)}Li·OEt2]2 (R = H or Me) with dimethylcyanamide and their reactive derivatives with metal halides.
• Authors of publication: Wang, Peng; Li, Haifen; Xue, Xiaoyan; Chen, Xia
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 10
• Pages of publication: 4718 - 4725
• a: 15.4886 ± 0.0007 Å
• b: 19.2519 ± 0.0009 Å
• c: 12.1325 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3617.7 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.0382
• Weighted residual factors for significantly intense reflections: 0.1021
• Weighted residual factors for all reflections included in the refinement: 0.1138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No