Information card for entry 7033994

Structure parameters

• Chemical name: {1,3-bis-(2,6-diisopropylphenyl)-1,3,2-diazaphospholenium}-triphenyl-stannyl-tricarbonyl ferrate(II)
• Formula: C47 H51 Fe N2 O3 P Sn
• Calculated formula: C47 H51 Fe N2 O3 P Sn
• Title of publication: An anionic phosphenium complex as an ambident nucleophile.
• Authors of publication: Stadelmann, B.; Bender, J.; Förster, D; Frey, W.; Nieger, M.; Gudat, D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 13
• Pages of publication: 6023 - 6031
• a: 11.5843 ± 0.0006 Å
• b: 12.234 ± 0.0006 Å
• c: 17.8887 ± 0.0011 Å
• α: 92.606 ± 0.003°
• β: 103.175 ± 0.003°
• γ: 116.117 ± 0.002°
• Cell volume: 2185.4 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0532
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0842
• Weighted residual factors for all reflections included in the refinement: 0.0919
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No