Information card for entry 7034063

Structure parameters

• Formula: C32 H46 B2 N O P2 S Si Sm
• Calculated formula: C32 H46 B2 N O P2 S Si Sm
• Title of publication: (Iminophosphoranyl)(thiophosphoranyl)methane rare-earth borohydride complexes: synthesis, structures and polymerization catalysis.
• Authors of publication: Schmid, Matthias; Oña-Burgos, Pascual; Guillaume, Sophie M.; Roesky, Peter W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 27
• Pages of publication: 12338 - 12348
• a: 12.863 ± 0.0005 Å
• b: 14.1648 ± 0.0005 Å
• c: 15.3321 ± 0.0006 Å
• α: 107.559 ± 0.003°
• β: 106.975 ± 0.003°
• γ: 96.833 ± 0.003°
• Cell volume: 2480.8 ± 0.18 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0514
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.1096
• Weighted residual factors for all reflections included in the refinement: 0.1135
• Goodness-of-fit parameter for all reflections included in the refinement: 0.99
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No