Information card for entry 7034308

Structure parameters

• Formula: C48 H88 Cl Li N4 O3.5 Si Zr
• Calculated formula: C48 H88 Cl Li N4 O3.5 Si Zr
• Title of publication: Synthesis, characterisation, and dehydrocoupling ability of zirconium complexes bearing hindered bis(amido)silyl ligands.
• Authors of publication: Lummis, Paul A.; McDonald, Robert; Ferguson, Michael J.; Rivard, Eric
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 15
• Pages of publication: 7009 - 7020
• a: 25.9179 ± 0.0011 Å
• b: 10.9638 ± 0.0005 Å
• c: 36.5714 ± 0.0015 Å
• α: 90°
• β: 90.0434 ± 0.0006°
• γ: 90°
• Cell volume: 10392.1 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0697
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.1145
• Weighted residual factors for all reflections included in the refinement: 0.1288
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No