Crystallography Open Database

Information card for entry 7034428

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Coordinates	7034428.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	h13msh17
Formula	C20 H58 B4 K2 N4 O3
Calculated formula	C20 H58 B4 K2 N4 O3
Title of publication	Alkali metal-mediated dehydrocoupling of Me2NH·BH3.
Authors of publication	Bellham, Peter; Hill, Michael S.; Kociok-Köhn, Gabriele
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	27
Pages of publication	12078 - 12081
a	12.5404 ± 0.0003 Å
b	17.0035 ± 0.0004 Å
c	15.9352 ± 0.0004 Å
α	90°
β	106.631 ± 0.0012°
γ	90°
Cell volume	3255.74 ± 0.14 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0699
Residual factor for significantly intense reflections	0.0424
Weighted residual factors for significantly intense reflections	0.0962
Weighted residual factors for all reflections included in the refinement	0.1096
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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