Information card for entry 7035033

Structure parameters

• Formula: C70 H65 B N2 O3 P2 Ru
• Calculated formula: C70 H65 B N2 O3 P2 Ru
• Title of publication: Preparation and reactivity of diazoalkane complexes of ruthenium stabilised by an indenyl ligand.
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; Dottorello, Gianluca
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 19
• Pages of publication: 9289 - 9303
• a: 15.3586 ± 0.0005 Å
• b: 17.5065 ± 0.0005 Å
• c: 22.5506 ± 0.0007 Å
• α: 90°
• β: 104.083 ± 0.0009°
• γ: 90°
• Cell volume: 5881.1 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0484
• Residual factor for significantly intense reflections: 0.0452
• Weighted residual factors for significantly intense reflections: 0.1273
• Weighted residual factors for all reflections included in the refinement: 0.1314
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No