Crystallography Open Database

Information card for entry 7035148

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Coordinates	7035148.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C185 H359 N17 O100 Si2 Ti4 W20
Calculated formula	C185 H359 N17 O100 Si2 Ti4 W20
Title of publication	Synthesis and structural characterization of BINOL-modified chiral polyoxometalates.
Authors of publication	Ishimoto, Ryo; Kamata, Keigo; Suzuki, Kosuke; Yamaguchi, Kazuya; Mizuno, Noritaka
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	24
Pages of publication	10947 - 10951
a	17.9204 ± 0.0003 Å
b	19.8114 ± 0.0003 Å
c	36.8133 ± 0.0005 Å
α	90°
β	90.0457 ± 0.0006°
γ	90°
Cell volume	13069.8 ± 0.3 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	7
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0619
Residual factor for significantly intense reflections	0.0546
Weighted residual factors for significantly intense reflections	0.1455
Weighted residual factors for all reflections included in the refinement	0.1539
Goodness-of-fit parameter for all reflections included in the refinement	1.081
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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