Information card for entry 7035368

Structure parameters

• Formula: C32 H34 Co3 Mo O9 P
• Calculated formula: C32 H34 Co3 Mo O9 P
• Title of publication: P-S bond cleavage in reactions of thiophosphinidene-bridged dimolybdenum complexes with [Co2(CO)8] to give phosphinidene-bridged heterometallic derivatives.
• Authors of publication: Alvarez, Belén; Alvarez, M. Angeles; García, M Esther; Ruiz, Miguel A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 1937 - 1952
• a: 9.9372 ± 0.0002 Å
• b: 15.6891 ± 0.0003 Å
• c: 10.8895 ± 0.0002 Å
• α: 90°
• β: 95.98 ± 0.002°
• γ: 90°
• Cell volume: 1688.5 ± 0.06 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0949
• Residual factor for significantly intense reflections: 0.0921
• Weighted residual factors for significantly intense reflections: 0.2325
• Weighted residual factors for all reflections included in the refinement: 0.2395
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No