Information card for entry 7035491

Structure parameters

• Formula: C26 H52 Cl6 N O8 Ru2
• Calculated formula: C26 H52 Cl6 N O8 Ru2
• Title of publication: An unprecedented up-field shift in the (13)C NMR spectrum of the carboxyl carbons of the lantern-type dinuclear complex TBA[Ru2(O2CCH3)4Cl2] (TBA(+) = tetra(n-butyl)ammonium cation).
• Authors of publication: Hiraoka, Yuya; Ikeue, Takahisa; Sakiyama, Hiroshi; Guégan, Frédéric; Luneau, Dominique; Gillon, Béatrice; Hiromitsu, Ichiro; Yoshioka, Daisuke; Mikuriya, Masahiro; Kataoka, Yusuke; Handa, Makoto
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 30
• Pages of publication: 13439 - 13443
• a: 11.9262 ± 0.0014 Å
• b: 12.4678 ± 0.0015 Å
• c: 13.3115 ± 0.0016 Å
• α: 76.86 ± 0.002°
• β: 82.601 ± 0.002°
• γ: 86.546 ± 0.002°
• Cell volume: 1910.5 ± 0.4 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0364
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0807
• Weighted residual factors for all reflections included in the refinement: 0.0832
• Goodness-of-fit parameter for all reflections included in the refinement: 0.908
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No