Information card for entry 7035815

Structure parameters

• Formula: C17 H32 F6 N2 P Sb
• Calculated formula: C17 H32 F6 N2 P Sb
• Title of publication: Synthesis and reactivity of α-cationic phosphines: the effect of imidazolinium and amidinium substituents.
• Authors of publication: Haldón, Estela; Kozma, Ágnes; Tinnermann, Hendrik; Gu, Lianghu; Goddard, Richard; Alcarazo, Manuel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 1872 - 1876
• a: 15.028 ± 0.003 Å
• b: 15.072 ± 0.003 Å
• c: 15.43 ± 0.003 Å
• α: 75.926 ± 0.003°
• β: 82.983 ± 0.003°
• γ: 74.157 ± 0.003°
• Cell volume: 3255.4 ± 1.1 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0674
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0854
• Weighted residual factors for all reflections included in the refinement: 0.1053
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No