Synthesis and characterisation of halide, separated ion pair, and hydride cyclopentadienyl iron bis(diphenylphosphino)ethane derivatives.
Authors of publication
Patel, Dipti; Wooles, Ashley; Cornish, Andrew D.; Steven, Lindsey; Davies, E. Stephen; Evans, David J.; McMaster, Jonathan; Lewis, William; Blake, Alexander J.; Liddle, Stephen T.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2015
Journal volume
44
Journal issue
31
Pages of publication
14159 - 14177
a
10.5992 ± 0.0009 Å
b
12.5015 ± 0.0011 Å
c
14.6903 ± 0.0013 Å
α
106.366 ± 0.001°
β
103.367 ± 0.001°
γ
104.021 ± 0.001°
Cell volume
1715.7 ± 0.3 Å3
Cell temperature
90 ± 2 K
Ambient diffraction temperature
90 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0391
Residual factor for significantly intense reflections
0.0331
Weighted residual factors for significantly intense reflections
0.0764
Weighted residual factors for all reflections included in the refinement
0.0803
Goodness-of-fit parameter for all reflections included in the refinement
