Information card for entry 7035887

Structure parameters

• Formula: C74 H105 Cl6 Dy5 O24 S4
• Calculated formula: C74 H100 Cl6 Dy5 O24 S4
• Title of publication: Pentanuclear lanthanide pyramids based on thiacalix[4]arene ligand exhibiting slow magnetic relaxation.
• Authors of publication: Ge, Jing-Yuan; Ru, Jing; Gao, Feng; Song, You; Zhou, Xin-Hui; Zuo, Jing-Lin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 35
• Pages of publication: 15481 - 15490
• a: 16.261 ± 0.004 Å
• b: 17.318 ± 0.004 Å
• c: 19.98 ± 0.005 Å
• α: 92.311 ± 0.004°
• β: 90.557 ± 0.004°
• γ: 111.324 ± 0.003°
• Cell volume: 5235 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0993
• Residual factor for significantly intense reflections: 0.0615
• Weighted residual factors for significantly intense reflections: 0.1769
• Weighted residual factors for all reflections included in the refinement: 0.2377
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No