Information card for entry 7035910

Structure parameters

• Chemical name: Rh_2_ppeb_4_THF
• Formula: C68 H32 F20 O10 Rh2
• Calculated formula: C68 H32 F20 O10 Rh2
• Title of publication: Porous frameworks constructed by non-covalent linking of substitution-inert metal complexes.
• Authors of publication: Itoh, Takahiro; Kondo, Mio; Sakamoto, Hirotoshi; Wakabayashi, Kaori; Kanaike, Mari; Itami, Kenichiro; Masaoka, Shigeyuki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 34
• Pages of publication: 15334 - 15342
• a: 18.64491 ± 0.00074 Å
• b: 27.22668 ± 0.0014 Å
• c: 8.89324 ± 0.00038 Å
• α: 90 ± 0°
• β: 107.482 ± 0.00123°
• γ: 90 ± 0°
• Cell volume: 4306 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0694
• Residual factor for significantly intense reflections: 0.066
• Weighted residual factors for significantly intense reflections: 0.1724
• Weighted residual factors for all reflections included in the refinement: 0.1742
• Goodness-of-fit parameter for all reflections included in the refinement: 1.135
• Diffraction radiation wavelength: 0.710747 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No