Information card for entry 7035934

Structure parameters

• Formula: C101 H90 Cl8 N2 P2 Si5
• Calculated formula: C101 H90 Cl8 N2 P2 Si5
• Title of publication: Extremely bulky secondary phosphinoamines as substituents for sterically hindered aminosilanes.
• Authors of publication: Böttcher, Tobias; Jones, Cameron
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 33
• Pages of publication: 14842 - 14853
• a: 17.441 ± 0.004 Å
• b: 23.78 ± 0.005 Å
• c: 23.866 ± 0.005 Å
• α: 90°
• β: 93.2 ± 0.03°
• γ: 90°
• Cell volume: 9883 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.168
• Residual factor for significantly intense reflections: 0.1007
• Weighted residual factors for significantly intense reflections: 0.2647
• Weighted residual factors for all reflections included in the refinement: 0.3063
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.7109 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No