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Information card for entry 7036019
Preview
Coordinates | 7036019.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C66 H90 N6 O2 Si2 |
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Calculated formula | C66 H90 N6 O2 Si2 |
SMILES | C1(c2ccccc2)=[N](c2c(cccc2C(C)C)C(C)C)[Si]2(N1c1c(C(C)C)cccc1C(C)C)(N(C)C)O[Si]1(O2)([N](=C(c2ccccc2)N1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)N(C)C |
Title of publication | Synthesis, structure and reactivity of a donor-stabilised silylene with a bulky bidentate benzamidinato ligand. |
Authors of publication | Tacke, Reinhold; Kobelt, Claudia; Baus, Johannes A.; Bertermann, Rüdiger; Burschka, Christian |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2015 |
Journal volume | 44 |
Journal issue | 33 |
Pages of publication | 14959 - 14974 |
a | 26.888 ± 0.004 Å |
b | 17.559 ± 0.002 Å |
c | 12.8562 ± 0.0018 Å |
α | 90° |
β | 93.712 ± 0.017° |
γ | 90° |
Cell volume | 6057 ± 1.4 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0954 |
Residual factor for significantly intense reflections | 0.038 |
Weighted residual factors for significantly intense reflections | 0.0748 |
Weighted residual factors for all reflections included in the refinement | 0.0869 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.802 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7036019.html
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