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Information card for entry 7036028
Preview
Coordinates | 7036028.cif |
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Original paper (by DOI) | HTML |
Formula | C33 H45 Cl2 N3 Si |
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Calculated formula | C33 H45 Cl2 N3 Si |
SMILES | Cl[Si]1(Cl)([N](=C(N1c1c(cccc1C(C)C)C(C)C)c1ccccc1)c1c(cccc1C(C)C)C(C)C)N(C)C |
Title of publication | Synthesis, structure and reactivity of a donor-stabilised silylene with a bulky bidentate benzamidinato ligand. |
Authors of publication | Tacke, Reinhold; Kobelt, Claudia; Baus, Johannes A.; Bertermann, Rüdiger; Burschka, Christian |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2015 |
Journal volume | 44 |
Journal issue | 33 |
Pages of publication | 14959 - 14974 |
a | 15.191 ± 0.0019 Å |
b | 15.191 ± 0.0019 Å |
c | 12.3499 ± 0.0018 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 2468.1 ± 0.6 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 144 |
Hermann-Mauguin space group symbol | P 31 |
Hall space group symbol | P 31 |
Residual factor for all reflections | 0.0612 |
Residual factor for significantly intense reflections | 0.047 |
Weighted residual factors for significantly intense reflections | 0.1102 |
Weighted residual factors for all reflections included in the refinement | 0.1178 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.971 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7036028.html
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