Information card for entry 7036035

Structure parameters

• Formula: C48 H50 Cl2 N2 P Sb
• Calculated formula: C48 H50 Cl2 N2 P Sb
• SMILES: [Sb]1(Cl)(Cl)[N](c2c(cccc2c2c(cc(cc2C)C)C)c2c(cc(cc2C)C)C)=PN1c1c(cccc1c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C
• Title of publication: Reduction of dichloro(diaza-phospha)stibanes - isolation of a donor-stabilized distibenium dication.
• Authors of publication: Hinz, Alexander; Rothe, Julia; Schulz, Axel; Villinger, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6044 - 6052
• a: 12.0987 ± 0.0009 Å
• b: 22.5405 ± 0.0018 Å
• c: 16.4923 ± 0.0014 Å
• α: 90°
• β: 106.879 ± 0.003°
• γ: 90°
• Cell volume: 4303.9 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1108
• Residual factor for significantly intense reflections: 0.0513
• Weighted residual factors for significantly intense reflections: 0.1075
• Weighted residual factors for all reflections included in the refinement: 0.1354
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No