Information card for entry 7036147

Structure parameters

• Formula: C39.2 H55.8 N12.6 O6 Pb
• Calculated formula: C39.166 H55.749 N12.583 O6 Pb
• Title of publication: Lanthanide(iii) and lead(ii) complexes of a chiral nonaaza macrocyclic amine based on 1,2-diaminocyclopentane.
• Authors of publication: Gregoliński, Janusz; Slepokura, Katarzyna; Lisowski, Jerzy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 37
• Pages of publication: 16345 - 16351
• a: 12.221 ± 0.003 Å
• b: 15.222 ± 0.003 Å
• c: 22.433 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4173.2 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0316
• Weighted residual factors for significantly intense reflections: 0.0528
• Weighted residual factors for all reflections included in the refinement: 0.0559
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No