Information card for entry 7036209

Structure parameters

• Formula: C42.5 H58 Lu N2 O P Si2
• Calculated formula: C42.5 H58 Lu N2 O P Si2
• Title of publication: Bis(alkyl) rare-earth complexes supported by a new tridentate amidinate ligand with a pendant diphenylphosphine oxide group. Synthesis, structures and catalytic activity in isoprene polymerization.
• Authors of publication: Tolpygin, Aleksei O.; Glukhova, Tatyana A.; Cherkasov, Anton V.; Fukin, Georgy K.; Aleksanyan, Diana V.; Cui, Dongmei; Trifonov, Alexander A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 37
• Pages of publication: 16465 - 16474
• a: 11.65759 ± 0.00019 Å
• b: 11.93192 ± 0.00015 Å
• c: 18.096 ± 0.0003 Å
• α: 74.6192 ± 0.0012°
• β: 72.6296 ± 0.0014°
• γ: 63.0777 ± 0.0014°
• Cell volume: 2116.79 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0297
• Residual factor for significantly intense reflections: 0.0243
• Weighted residual factors for significantly intense reflections: 0.0504
• Weighted residual factors for all reflections included in the refinement: 0.0516
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No