Information card for entry 7036294

Structure parameters

• Formula: C22 H22 N5 O15 Sm Zn
• Calculated formula: C22 H22 N5 O15 Sm Zn
• Title of publication: Spectroscopic studies of lanthanide complexes of varying nuclearity based on a compartmentalised ligand.
• Authors of publication: Olea-Román, Daniela; Bélanger-Desmarais, Nicolas; Flores-Álamo, Marcos; Bazán, Claudia; Thouin, Félix; Reber, Christian; Castillo-Blum, Silvia E
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 39
• Pages of publication: 17175 - 17188
• a: 9.7146 ± 0.0014 Å
• b: 12.1476 ± 0.0013 Å
• c: 12.9509 ± 0.0006 Å
• α: 83.09 ± 0.007°
• β: 71.598 ± 0.01°
• γ: 87.232 ± 0.01°
• Cell volume: 1439.6 ± 0.3 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0465
• Residual factor for significantly intense reflections: 0.0352
• Weighted residual factors for significantly intense reflections: 0.0711
• Weighted residual factors for all reflections included in the refinement: 0.0772
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No