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Information card for entry 7036299
Preview
Coordinates | 7036299.cif |
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Original paper (by DOI) | HTML |
Formula | C21 H32 N O P Sn |
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Calculated formula | C21 H32 N O P Sn |
SMILES | O=[P@](c1c([Sn](C)(C)C)cccc1)(N[C@@H](C)C(C)(C)C)c1ccccc1 |
Title of publication | Synthesis of P-stereogenic diarylphosphinic amides by directed lithiation: transformation into tertiary phosphine oxides via methanolysis, aryne chemistry and complexation behaviour toward zinc(ii). |
Authors of publication | Del Águila-Sánchez, Miguel A; Navarro, Yolanda; García López, Jesús; Guedes, Guilherme P.; López Ortiz, Fernando |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 5 |
Pages of publication | 2008 - 2022 |
a | 9.3648 ± 0.0002 Å |
b | 9.3648 ± 0.0002 Å |
c | 51.2257 ± 0.0012 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 4492.47 ± 0.17 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 96 |
Hermann-Mauguin space group symbol | P 43 21 2 |
Hall space group symbol | P 4nw 2abw |
Residual factor for all reflections | 0.0535 |
Residual factor for significantly intense reflections | 0.0528 |
Weighted residual factors for significantly intense reflections | 0.1369 |
Weighted residual factors for all reflections included in the refinement | 0.1376 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7036299.html
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