Information card for entry 7036321

Structure parameters

• Formula: C36 H58 P4
• Calculated formula: C35.991 H57.973 P4
• Title of publication: Synthetic strategies to bicyclic tetraphosphanes using P1, P2 and P4 building blocks.
• Authors of publication: Bresien, Jonas; Faust, Kirill; Hering-Junghans, Christian; Rothe, Julia; Schulz, Axel; Villinger, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 1998 - 2007
• a: 16.7738 ± 0.0004 Å
• b: 10.7853 ± 0.0002 Å
• c: 20.6732 ± 0.0005 Å
• α: 90°
• β: 95.943 ± 0.001°
• γ: 90°
• Cell volume: 3719.9 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0801
• Residual factor for significantly intense reflections: 0.0499
• Weighted residual factors for significantly intense reflections: 0.1181
• Weighted residual factors for all reflections included in the refinement: 0.1346
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No