Information card for entry 7036325

Structure parameters

• Formula: C43 H66 Cl3 Ga P4
• Calculated formula: C43 H66 Cl3 Ga P4
• Title of publication: Synthetic strategies to bicyclic tetraphosphanes using P1, P2 and P4 building blocks.
• Authors of publication: Bresien, Jonas; Faust, Kirill; Hering-Junghans, Christian; Rothe, Julia; Schulz, Axel; Villinger, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 1998 - 2007
• a: 13.2689 ± 0.0004 Å
• b: 12.9252 ± 0.0005 Å
• c: 14.1556 ± 0.0005 Å
• α: 90°
• β: 90.676 ± 0.002°
• γ: 90°
• Cell volume: 2427.56 ± 0.15 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0716
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.0823
• Weighted residual factors for all reflections included in the refinement: 0.0945
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No