Information card for entry 7036454

Structure parameters

• Formula: C32 H45 Ga N2 O1.77
• Calculated formula: C32 H45 Ga N2 O1.772
• Title of publication: Synthesis of substituted β-diketiminate gallium hydrides via oxidative addition of H-O bonds.
• Authors of publication: Herappe-Mejía, Eduardo; Trujillo-Hernández, Karla; Carlos Garduño-Jiménez, Juan; Cortés-Guzmán, Fernando; Martínez-Otero, Diego; Jancik, Vojtech
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 38
• Pages of publication: 16894 - 16902
• a: 12.0219 ± 0.0006 Å
• b: 28.9891 ± 0.0013 Å
• c: 8.9674 ± 0.0004 Å
• α: 90°
• β: 98.879 ± 0.001°
• γ: 90°
• Cell volume: 3087.7 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0388
• Residual factor for significantly intense reflections: 0.0311
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0782
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No