Information card for entry 7036487

Structure parameters

• Formula: C48 H43 B F18 P2 Rh
• Calculated formula: C45 H36 B F18 P2 Rh
• Title of publication: Transition metal-mediated donor-acceptor coordination of low-oxidation state Group 14 element halides.
• Authors of publication: Swarnakar, Anindya K.; Ferguson, Michael J.; McDonald, Robert; Rivard, Eric
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6071 - 6078
• a: 12.2135 ± 0.0003 Å
• b: 12.5991 ± 0.0003 Å
• c: 17.0103 ± 0.0004 Å
• α: 80.6961 ± 0.001°
• β: 81.3382 ± 0.0008°
• γ: 75.25 ± 0.0008°
• Cell volume: 2481.49 ± 0.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0323
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.0855
• Weighted residual factors for all reflections included in the refinement: 0.086
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No