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Information card for entry 7036599
Preview
Coordinates | 7036599.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C15 H20 Cl P |
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Calculated formula | C15 H20 Cl P |
SMILES | ClP(C#CC(C)(C)C)c1c(C)cc(C)cc1C |
Title of publication | Hydroalumination of alkynyl-aminophosphines as a promising tool for the synthesis of unusual phosphines: P-N bond activation, a transient phosphaallene, a zwitterionic AlP2C2 heterocycle and a masked Al/P-based frustrated Lewis pair. |
Authors of publication | Klöcker, Hans; Layh, Marcus; Hepp, Alexander; Uhl, Werner |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 5 |
Pages of publication | 2031 - 2043 |
a | 8.8446 ± 0.0005 Å |
b | 13.6377 ± 0.0011 Å |
c | 12.7896 ± 0.001 Å |
α | 90° |
β | 95.263 ± 0.003° |
γ | 90° |
Cell volume | 1536.18 ± 0.19 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0847 |
Residual factor for significantly intense reflections | 0.0546 |
Weighted residual factors for significantly intense reflections | 0.1391 |
Weighted residual factors for all reflections included in the refinement | 0.155 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7036599.html
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