Information card for entry 7036616

Structure parameters

• Formula: C36 H50 N4 Ni O2
• Calculated formula: C36 H50 N4 Ni O2
• Title of publication: X-ray structure of a Ni(ii)-tri-phenoxyl radical complex.
• Authors of publication: Benisvy, Laurent; Zats, Galina M.; Fleker, Ohad; Yufit, Dmitry S.; Orio, Maylis; Romanenko, Galina; Ovcharenko, Victor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 41
• Pages of publication: 17924 - 17926
• a: 17.361 ± 0.0006 Å
• b: 10.3225 ± 0.0004 Å
• c: 9.2567 ± 0.0003 Å
• α: 90°
• β: 92.41 ± 0.01°
• γ: 90°
• Cell volume: 1657.42 ± 0.1 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0639
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.1121
• Weighted residual factors for all reflections included in the refinement: 0.1261
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MOKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No