Information card for entry 7036648

Structure parameters

• Formula: C33 H50 Cl4 Ga N3 P2
• Calculated formula: C33 H50 Cl4 Ga N3 P2
• Title of publication: From the parent phosphinidene-carbene adduct NHC[double bond, length as m-dash]PH to cationic P4-rings and P2-cycloaddition products.
• Authors of publication: Beil, Andreas; Gilliard, Robert J.; Grützmacher, Hansjörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 2044 - 2052
• a: 10.3933 ± 0.0008 Å
• b: 24.7035 ± 0.0017 Å
• c: 15.9464 ± 0.0012 Å
• α: 90°
• β: 105.836 ± 0.004°
• γ: 90°
• Cell volume: 3938.9 ± 0.5 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0511
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0708
• Weighted residual factors for all reflections included in the refinement: 0.0769
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No