Information card for entry 7036651

Structure parameters

• Formula: C39 H60 Cl4 Ga N3 P2
• Calculated formula: C39 H60 Cl4 Ga N3 P2
• Title of publication: From the parent phosphinidene-carbene adduct NHC[double bond, length as m-dash]PH to cationic P4-rings and P2-cycloaddition products.
• Authors of publication: Beil, Andreas; Gilliard, Robert J.; Grützmacher, Hansjörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 2044 - 2052
• a: 10.7703 ± 0.0002 Å
• b: 15.0762 ± 0.0003 Å
• c: 27.5758 ± 0.0005 Å
• α: 90°
• β: 101.072 ± 0.001°
• γ: 90°
• Cell volume: 4394.28 ± 0.14 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0487
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0908
• Weighted residual factors for all reflections included in the refinement: 0.0981
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No