Information card for entry 7036776

Structure parameters

• Formula: C88 H118 N2 Nb2 O6 P6
• Calculated formula: C94 H124 N2 Nb2 O6 P6
• Title of publication: Assembly and stabilization of {E(cyclo-P3)2} (E = Sn, Pb) as a bridging ligand spanning two triaryloxyniobium units.
• Authors of publication: Velian, Alexandra; Cossairt, Brandi M.; Cummins, Christopher C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 1891 - 1895
• a: 10.4029 ± 0.0007 Å
• b: 13.7294 ± 0.001 Å
• c: 16.3434 ± 0.0012 Å
• α: 94.929 ± 0.001°
• β: 93.683 ± 0.001°
• γ: 95.884 ± 0.001°
• Cell volume: 2307.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0837
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.0829
• Weighted residual factors for all reflections included in the refinement: 0.0982
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No