Information card for entry 7036781

Structure parameters

• Formula: C48.8 H69.19 Nb O4 P3 Pb0.5
• Calculated formula: C48.8 H69.2 Nb O4 P3 Pb0.5
• Title of publication: Assembly and stabilization of {E(cyclo-P3)2} (E = Sn, Pb) as a bridging ligand spanning two triaryloxyniobium units.
• Authors of publication: Velian, Alexandra; Cossairt, Brandi M.; Cummins, Christopher C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 1891 - 1895
• a: 23.9973 ± 0.0014 Å
• b: 12.5011 ± 0.0007 Å
• c: 33.949 ± 0.002 Å
• α: 90°
• β: 102.473 ± 0.001°
• γ: 90°
• Cell volume: 9944.1 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0321
• Residual factor for significantly intense reflections: 0.0271
• Weighted residual factors for significantly intense reflections: 0.0569
• Weighted residual factors for all reflections included in the refinement: 0.0585
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No