Microwave gallium-68 radiochemistry for kinetically stable bis(thiosemicarbazone) complexes: structural investigations and cellular uptake under hypoxia.
Authors of publication
Alam, Israt S.; Arrowsmith, Rory L.; Cortezon-Tamarit, Fernando; Twyman, Frazer; Kociok-Köhn, Gabriele; Botchway, Stanley W.; Dilworth, Jonathan R.; Carroll, Laurence; Aboagye, Eric O.; Pascu, Sofia I.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2015
Journal volume
45
Journal issue
1
Pages of publication
144 - 155
a
7.859 ± 0.007 Å
b
11.04 ± 0.009 Å
c
12.049 ± 0.009 Å
α
90.546 ± 0.006°
β
95.388 ± 0.001°
γ
110.304 ± 0.013°
Cell volume
975.1 ± 1.4 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0802
Residual factor for significantly intense reflections
0.0573
Weighted residual factors for significantly intense reflections
0.1398
Weighted residual factors for all reflections included in the refinement
0.151
Goodness-of-fit parameter for all reflections included in the refinement
