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Information card for entry 7036994
Preview
Coordinates | 7036994.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C54 H84 N6 Si4 Sm2 |
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Calculated formula | C54 H84 N6 Si4 Sm2 |
SMILES | [C]123=[CH]4[Sm]56782([N]1([Sm]129%10(N(C3)c3c(cccc3C(C)C)C(C)C)([N]36[C]1(=[CH]2[C]19C=CC=C[C]%103=1)CN7c1c(cccc1C(C)C)C(C)C)N([Si](C)(C)C)[Si](C)(C)C)[C]18=[C]45C=CC=C1)N([Si](C)(C)C)[Si](C)(C)C |
Title of publication | Reactivity of functionalized indoles with rare-earth metal amides. Synthesis, characterization and catalytic activity of rare-earth metal complexes incorporating indolyl ligands. |
Authors of publication | Feng, Zhijun; Wei, Yun; Zhou, Shuangliu; Zhang, Guangchao; Zhu, Xiancui; Guo, Liping; Wang, Shaowu; Mu, Xiaolong |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2015 |
Journal volume | 44 |
Journal issue | 47 |
Pages of publication | 20502 - 20513 |
a | 9.814 ± 0.003 Å |
b | 15.222 ± 0.004 Å |
c | 21.286 ± 0.006 Å |
α | 73.257 ± 0.003° |
β | 86.632 ± 0.003° |
γ | 77.623 ± 0.003° |
Cell volume | 2974.3 ± 1.5 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0932 |
Residual factor for significantly intense reflections | 0.0614 |
Weighted residual factors for significantly intense reflections | 0.1575 |
Weighted residual factors for all reflections included in the refinement | 0.1793 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7036994.html
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Users of the data should acknowledge the original authors of the
structural data.