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Information card for entry 7037050
Preview
Coordinates | 7037050.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | As3 Na15 O169 U6 W27 |
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Calculated formula | As3 Na15 O169 U6 W27 |
Title of publication | B-α-[AsW9O33](9-) polyoxometalates incorporating hexanuclear uranium {U6O8}-like clusters bearing the U(IV) form or unprecedented mixed valence U(IV)/U(VI) involving direct U(VI)[double bond, length as m-dash]O-U(IV) bonding. |
Authors of publication | Duval, Sylvain; Sobanska, Sophie; Roussel, Pascal; Loiseau, Thierry |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2015 |
Journal volume | 44 |
Journal issue | 46 |
Pages of publication | 19772 - 19776 |
a | 13.7846 ± 0.0008 Å |
b | 31.0033 ± 0.0014 Å |
c | 17.7568 ± 0.0008 Å |
α | 90° |
β | 91.543 ± 0.003° |
γ | 90° |
Cell volume | 7585.9 ± 0.7 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100.03 K |
Number of distinct elements | 5 |
Space group number | 11 |
Hermann-Mauguin space group symbol | P 1 21/m 1 |
Hall space group symbol | -P 2yb |
Residual factor for all reflections | 0.0696 |
Residual factor for significantly intense reflections | 0.038 |
Weighted residual factors for significantly intense reflections | 0.0798 |
Weighted residual factors for all reflections included in the refinement | 0.0934 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7037050.html
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