Information card for entry 7037057

Structure parameters

• Formula: C30 H45 Cl2 N3 Si
• Calculated formula: C30 H45 Cl2 N3 Si
• Title of publication: Base-stabilized silaimine and its donor-free dimer derived from the reaction of NHC-supported silylene with SiCl4.
• Authors of publication: Cui, Haiyan; Cui, Chunming
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 47
• Pages of publication: 20326 - 20329
• a: 9.49 ± 0.004 Å
• b: 14.842 ± 0.006 Å
• c: 21.882 ± 0.009 Å
• α: 90°
• β: 91.321 ± 0.007°
• γ: 90°
• Cell volume: 3081 ± 2 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 113 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0825
• Residual factor for significantly intense reflections: 0.0656
• Weighted residual factors for significantly intense reflections: 0.1669
• Weighted residual factors for all reflections included in the refinement: 0.1781
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No