Information card for entry 7037150

Structure parameters

• Formula: C43 H36 B F10 P
• Calculated formula: C43 H36 B F10 P
• Title of publication: Unusual borane addition to conjugated dienylphosphanes under frustrated Lewis pair conditions.
• Authors of publication: Krupski, Sergei; Kehr, Gerald; Daniliuc, Constantin G.; Erker, Gerhard
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6111 - 6117
• a: 11.2806 ± 0.0004 Å
• b: 12.2184 ± 0.0004 Å
• c: 17.13 ± 0.0008 Å
• α: 75.251 ± 0.001°
• β: 78.781 ± 0.001°
• γ: 88.548 ± 0.003°
• Cell volume: 2238.89 ± 0.15 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1743
• Residual factor for significantly intense reflections: 0.1011
• Weighted residual factors for significantly intense reflections: 0.2763
• Weighted residual factors for all reflections included in the refinement: 0.3124
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No