Information card for entry 7037200

Structure parameters

• Formula: C15.6 H30.4 F6 Ge N4.8 O6 S2
• Calculated formula: C15.6 H30.4 F6 Ge N4.8 O6 S2
• Title of publication: Cationic aza-macrocyclic complexes of germanium(ii) and silicon(iv).
• Authors of publication: Everett, Matthew; Jolleys, Andrew; Levason, William; Light, Mark E.; Pugh, David; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 48
• Pages of publication: 20898 - 20905
• a: 17.1253 ± 0.0003 Å
• b: 17.1253 ± 0.0003 Å
• c: 22.116 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6486.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 103
• Hermann-Mauguin space group symbol: P 4 c c
• Hall space group symbol: P 4 -2c
• Residual factor for all reflections: 0.0708
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.1312
• Weighted residual factors for all reflections included in the refinement: 0.1418
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No