Information card for entry 7037202

Structure parameters

• Formula: C11 H24 Cl2 Ge N4
• Calculated formula: C11 H24 Cl2 Ge N4
• SMILES: C1C[N]2(CC[N]3(CC[N]1(C)[Ge]23)C)C.C(#N)C.[Cl-].[Cl-]
• Title of publication: Cationic aza-macrocyclic complexes of germanium(ii) and silicon(iv).
• Authors of publication: Everett, Matthew; Jolleys, Andrew; Levason, William; Light, Mark E.; Pugh, David; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 48
• Pages of publication: 20898 - 20905
• a: 14.399 ± 0.005 Å
• b: 10.139 ± 0.005 Å
• c: 21.491 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3138 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.1075
• Residual factor for significantly intense reflections: 0.0608
• Weighted residual factors for significantly intense reflections: 0.1029
• Weighted residual factors for all reflections included in the refinement: 0.119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No