Information card for entry 7037204

Structure parameters

• Formula: C9.67 H22.33 Cl5.33 N3 Si
• Calculated formula: C9.66667 H22.3333 Cl5.33333 N3 Si
• Title of publication: Cationic aza-macrocyclic complexes of germanium(ii) and silicon(iv).
• Authors of publication: Everett, Matthew; Jolleys, Andrew; Levason, William; Light, Mark E.; Pugh, David; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 48
• Pages of publication: 20898 - 20905
• a: 34.475 ± 0.008 Å
• b: 26.707 ± 0.006 Å
• c: 11.82 ± 0.003 Å
• α: 90°
• β: 106.684 ± 0.005°
• γ: 90°
• Cell volume: 10425 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1207
• Residual factor for significantly intense reflections: 0.0943
• Weighted residual factors for significantly intense reflections: 0.2271
• Weighted residual factors for all reflections included in the refinement: 0.2472
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No