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Information card for entry 7037417
Preview
Coordinates | 7037417.cif |
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Original paper (by DOI) | HTML |
Formula | C32 H20 B Cl3 Cu F9 N6 |
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Calculated formula | C32 H20 B Cl3 Cu F9 N6 |
Title of publication | Highly tunable fluorinated trispyrazolylborates [HB(3-CF3-5-{4-RPh}pz)3](-) (R = NO2, CF3, Cl, F, H, OMe and NMe2) and their copper(i) complexes. |
Authors of publication | van Dijkman, Thomas F.; Siegler, Maxime A.; Bouwman, Elisabeth |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2015 |
Journal volume | 44 |
Journal issue | 48 |
Pages of publication | 21109 - 21123 |
a | 17.33337 ± 0.00013 Å |
b | 14.29443 ± 0.00011 Å |
c | 27.0397 ± 0.00018 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 6699.64 ± 0.08 Å3 |
Cell temperature | 110 ± 2 K |
Ambient diffraction temperature | 110 ± 2 K |
Number of distinct elements | 7 |
Space group number | 29 |
Hermann-Mauguin space group symbol | P c a 21 |
Hall space group symbol | P 2c -2ac |
Residual factor for all reflections | 0.0353 |
Residual factor for significantly intense reflections | 0.0342 |
Weighted residual factors for significantly intense reflections | 0.0938 |
Weighted residual factors for all reflections included in the refinement | 0.0947 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7037417.html
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