Crystallography Open Database

Information card for entry 7037608

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Coordinates	7037608.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H43 Mn N2 O4
Calculated formula	C33 H43 Mn N2 O4
Title of publication	Stabilisation of carbonyl free amidinato-manganese(ii) hydride complexes: "masked" sources of manganese(i) in organometallic synthesis.
Authors of publication	Fohlmeister, Lea; Jones, Cameron
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	4
Pages of publication	1436 - 1442
a	9.5137 ± 0.0004 Å
b	10.4772 ± 0.0005 Å
c	17.1114 ± 0.0008 Å
α	85.869 ± 0.004°
β	83.117 ± 0.004°
γ	67.869 ± 0.004°
Cell volume	1567.89 ± 0.13 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0785
Residual factor for significantly intense reflections	0.0544
Weighted residual factors for significantly intense reflections	0.1217
Weighted residual factors for all reflections included in the refinement	0.1364
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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