Information card for entry 7037615

Structure parameters

• Formula: C52 H60 N Ni O2 P
• Calculated formula: C52 H60 N Ni O2 P
• Title of publication: Ethylene polymerization by salicylaldimine nickel(ii) complexes containing a dibenzhydryl moiety.
• Authors of publication: Hu, Xiaohui; Dai, Shengyu; Chen, Changle
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 4
• Pages of publication: 1496 - 1503
• a: 10.8638 ± 0.0003 Å
• b: 16.9433 ± 0.0004 Å
• c: 25.4176 ± 0.0005 Å
• α: 90°
• β: 98.39 ± 0.002°
• γ: 90°
• Cell volume: 4628.51 ± 0.19 ų
• Cell temperature: 290 ± 2 K
• Ambient diffraction temperature: 290 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0757
• Residual factor for significantly intense reflections: 0.0554
• Weighted residual factors for significantly intense reflections: 0.1495
• Weighted residual factors for all reflections included in the refinement: 0.1665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No