Information card for entry 7037765

Structure parameters

• Formula: C50 H37 Dy2 F36 I N4 O16
• Calculated formula: C50 H37 Dy2 F36 I N4 O16
• Title of publication: First coordination compounds based on a bis(imino nitroxide) biradical and 4f metal ions: synthesis, crystal structures and magnetic properties.
• Authors of publication: Reis, Samira G.; Briganti, Matteo; Martins, Daniel O. T. A.; Akpinar, Handan; Calancea, Sergiu; Guedes, Guilherme P.; Soriano, Stéphane; Andruh, Marius; Cassaro, Rafael A. A.; Lahti, Paul M.; Totti, Federico; Vaz, Maria G. F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 7
• Pages of publication: 2936 - 2944
• a: 12.5244 ± 0.0008 Å
• b: 13.2968 ± 0.0009 Å
• c: 23.3803 ± 0.0016 Å
• α: 89.62 ± 0.006°
• β: 83.29 ± 0.006°
• γ: 65.009 ± 0.007°
• Cell volume: 3501 ± 0.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1293
• Residual factor for significantly intense reflections: 0.0822
• Weighted residual factors for significantly intense reflections: 0.2082
• Weighted residual factors for all reflections included in the refinement: 0.2596
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No