Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7037771
Preview
Coordinates | 7037771.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C50 H39 F3 P2 Ru |
---|---|
Calculated formula | C50 H39 F3 P2 Ru |
Title of publication | Access to novel fluorovinylidene ligands via exploitation of outer-sphere electrophilic fluorination: new insights into C-F bond formation and activation. |
Authors of publication | Milner, Lucy M.; Hall, Lewis M.; Pridmore, Natalie E.; Skeats, Matthew K.; Whitwood, Adrian C.; Lynam, Jason M.; Slattery, John M. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 4 |
Pages of publication | 1717 - 1726 |
a | 16.8756 ± 0.0003 Å |
b | 15.1925 ± 0.0002 Å |
c | 17.3468 ± 0.0004 Å |
α | 90° |
β | 116.921 ± 0.003° |
γ | 90° |
Cell volume | 3965.46 ± 0.16 Å3 |
Cell temperature | 110 ± 0.14 K |
Ambient diffraction temperature | 110 ± 0.14 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0437 |
Residual factor for significantly intense reflections | 0.0324 |
Weighted residual factors for significantly intense reflections | 0.0724 |
Weighted residual factors for all reflections included in the refinement | 0.0781 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.052 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71071 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7037771.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.