Information card for entry 7037831

Structure parameters

• Formula: C90 H130 Li2 N4 O8 Sn2
• Calculated formula: C90 H130 Li2 N4 O8 Sn2
• Title of publication: Synthesis and reactivity of fluorenyl-tethered N-heterocyclic stannylenes.
• Authors of publication: Roselló-Merino, Marta; Mansell, Stephen M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6282 - 6293
• a: 10.0025 ± 0.0004 Å
• b: 26.2852 ± 0.0011 Å
• c: 16.4291 ± 0.0006 Å
• α: 90°
• β: 97.9963 ± 0.0016°
• γ: 90°
• Cell volume: 4277.5 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0344
• Weighted residual factors for significantly intense reflections: 0.0626
• Weighted residual factors for all reflections included in the refinement: 0.0678
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No