Information card for entry 7037834

Structure parameters

• Formula: C74 H90 N4 Rh2 Sn2
• Calculated formula: C74 H90 N4 Rh2 Sn2
• SMILES: [c]12([c]34[c]5([c]67[c]1(cccc6)[Rh]1682457[CH]2=[CH]1CC[CH]6=[CH]8CC2)cccc3)CC[N]12CCN(c3c(cccc3C(C)C)C(C)C)[Sn]1[N]1(CC[c]34[c]56[c]7(cccc5)[c]58[c]3(cccc5)[Rh]3594678[CH]4=[CH]3CC[CH]5=[CH]9CC4)CCN(c3c(cccc3C(C)C)C(C)C)[Sn]21
• Title of publication: Synthesis and reactivity of fluorenyl-tethered N-heterocyclic stannylenes.
• Authors of publication: Roselló-Merino, Marta; Mansell, Stephen M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6282 - 6293
• a: 8.63 ± 0.0008 Å
• b: 30.633 ± 0.003 Å
• c: 11.9259 ± 0.001 Å
• α: 90°
• β: 101.213 ± 0.005°
• γ: 90°
• Cell volume: 3092.6 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1663
• Residual factor for significantly intense reflections: 0.1046
• Weighted residual factors for significantly intense reflections: 0.238
• Weighted residual factors for all reflections included in the refinement: 0.2656
• Goodness-of-fit parameter for all reflections included in the refinement: 1.11
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No